Analytical Chemistry. Plenary Lectures Presented at the by A. Hulanicki

By A. Hulanicki

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Mechanized bubbler devices are used to collect sulphur dioxide, nitrogen dioxide, mercury, and other gases and vapours. These samplers, although typically designed for collecting 24 h integrated samples, can be modified to collect 1 or 2 h samples in sequence, and thus allow definition of diurnal variations. In automatic sampler-analysers, collection and analysis are combined in a single device. These automatic instruments produce continuous analysis, with the output in a machine-readable format or in a form suitable for telemetry to a central data-acquisition facility.

Consequently it remains difficult to distinguish between a genuine difference in total body calcium and a redistribution of calcium within the body. Furthermore the conversion ratio between 4 9 Ca counts and total body calcium varies according to the size and shape of the patient and cannot be standardized. The same considerations restrict the usefulness of activation analysis in estimating the total body content of other elements. THYROID IODINE Activation analysis of limited regions of the body presents less formidable problems: The thyroid gland is an obvious target for work of this kind, since it contains a substantial part of the body's total iodine.

M ed. 9, 110 (1968). K. Boddy, R. M. Harden and W. D. Alexander, J. Clin. Endocrinol. Metab. 28, 294 (1964). B. Carlmark and P. Reizenstein, in reference 5, p 113. H. E. Palmer and W. B. Nelp, in reference 5, p 127. G. J. Peterson, in Nuclear Activation Techniques in the Life Sciences, p 323. IAEA: Vienna (1972). J. S. Orr and F. C. Gillespie, Science, 162, 138 (1969). F. C. Gillespie, J. Shimmins and J. M. A. Lenihan, Radiochem. Radioanal. Letters, 4,43 (1970). B. Maziere, M. Maziere and D. Cornar, in Nuclear Activation Techniques in the Life Sciences, p 359.

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